Step |
Time (min) |
Water |
Methanol |
0 |
0.0 |
80 % |
20 % |
1 |
2.0 |
80 % |
20 % |
2 |
7.0 |
52 % |
48 % |
3 |
10.0 |
50 % |
50 % |
4 |
15.0 |
47 % |
53 % |
5 |
20.0 |
42 % |
58 % |
6 |
24.0 |
35 % |
65 % |
7 |
32.0 |
25 % |
75 % |
8 |
35.0 |
10 % |
90 % |
9 |
35.1 |
0 % |
100 % |
10 |
40.0 |
0 % |
100 % |
11 |
40.1 |
80 % |
20 % |
12 |
52.0 |
80 % |
20 % |