Analyte |
IS reference |
Peak distance (min) |
Accuracy |
RSD |
RL (ng/g) |
Male
conc. (ng/g) |
Female conc. (ng/g) |
SRM conc. (ng/g) |
Curve |
R2 |
Slope |
17OHP4
|
17OHP4-13C3 |
— |
106.83 |
1.507 |
0.2088 |
0.3508 |
0.4586 |
3.195 |
low |
0.9999 |
0.0646 |
|
|
|
|
|
|
|
|
|
high |
0.9990 |
0.0599 |
|
T-13C3
|
0.19 |
97.96 |
4.315 |
0.1112 |
0.2560 |
0.3208 |
3.628 |
low |
0.9999 |
0.4976 |
|
|
|
|
|
|
|
|
|
high |
0.9997 |
0.5613 |
|
AE-13C3
|
2.37 |
108.87 |
1.404 |
0.1056 |
0.1600 |
0.2868 |
3.075 |
low |
0.9999 |
0.7898 |
|
|
|
|
|
|
|
|
|
high |
1.0000 |
0.0639 |
|
P4-13C3
|
3.71 |
222.00 |
59.909 |
0.1056 |
0.4575 |
0.8876 |
10.945 |
low |
0.9999 |
0.1907 |
|
|
|
|
|
|
|
|
|
high |
1.0000 |
0.1976 |
T |
T-13C3 |
— |
110.49 |
1.633 |
0.1505 |
4.878 |
<LOQ |
<LOQ |
low |
1.0000 |
1.1497 |
|
|
|
|
|
|
|
|
|
high |
1.0000 |
1.1493 |
|
17OHP4-13C3
|
0.19 |
110.08 |
3.730 |
0.1505 |
5.721 |
<LOQ |
<LOQ |
low |
0.9999 |
0.1492 |
|
|
|
|
|
|
|
|
|
high |
0.9999 |
0.1493 |
|
AE-13C3
|
2.19 |
120.59 |
26.390 |
0.1505 |
4.955 |
<LOQ |
<LOQ |
low |
0.9998 |
2.1209 |
|
|
|
|
|
|
|
|
|
high |
0.9996 |
1.8151 |
|
P4-13C3
|
3.53 |
231.69 |
55.585 |
0.1505 |
7.339 |
<LOQ |
<LOQ |
low |
1.0000 |
0.4616 |
|
|
|
|
|
|
|
|
|
high |
0.9999 |
0.4398 |
AE |
AE-13C3 |
— |
107.23 |
1.818 |
1.260 |
10.514 |
12.97 |
11.120 |
low |
0.9999 |
0.2268 |
|
|
|
|
|
|
|
|
|
high |
1.0000 |
0.2218 |
|
P4-C3 |
1.35 |
186.23 |
29.194 |
1.260 |
14.287 |
22.35 |
22.217 |
low |
1.0000 |
0.0530 |
|
|
|
|
|
|
|
|
|
high |
1.0000 |
0.0523 |
|
T-13C3
|
2.18 |
99.41 |
18.897 |
1.260 |
9.693 |
10.86 |
9.180 |
low |
0.9998 |
0.1381 |
|
|
|
|
|
|
|
|
|
high |
0.9999 |
0.1483 |
|
17OHP4-13C3
|
2.37 |
106.94 |
21.040 |
1.260 |
11.169 |
13.15 |
8.566 |
low |
1.0000 |
0.0169 |
|
|
|
|
|
|
|
|
|
high |
0.9993 |
0.0178 |
P4
|
P4-13C3 |
— |
107.42 |
5.236 |
0.07101 |
0.3653 |
112.20 |
348.7 |
low |
0.9999 |
0.5318 |
|
|
|
|
|
|
|
|
|
high |
0.9995 |
0.4732 |
|
AE-13C3
|
1.34 |
108.53 |
5.272 |
0.07101 |
0.2320 |
114.40 |
351.6 |
low |
1.0000 |
2.2952 |
|
|
|
|
|
|
|
|
|
high |
1.0000 |
0.4725 |
|
T-13C3
|
3.52 |
71.91 |
27.888 |
0.07101 |
0.2544 |
46.37 |
115.1 |
low |
1.0000 |
1.3282 |
|
|
|
|
|
|
|
|
|
high |
1.0000 |
1.4811 |
|
17OHP4-13C3
|
3.71 |
77.08 |
34.630 |
0.07101 |
0.2625 |
64.16 |
139.2 |
low |
1.0000 |
0.1740 |
|
|
|
|
|
|
|
|
|
high |
0.9998 |
0.1590 |