Analyte |
IS reference |
Peak distance (min) |
Accuracy |
RSD |
RL (ng/g) |
Male
(ng/g) |
Female (ng/g) |
SRM (ng/g) |
R2 |
Slope |
ALD |
Ald-d4 |
— |
88.96 |
9.159 |
3.539 |
<RL |
<RL |
<RL |
0.9994 |
1.1725 |
|
E-13C3
|
1.59 |
69.29 |
12.43 |
3.539 |
<RL |
<RL |
<RL |
0.9337 |
0.1715 |
|
F-13C3
|
3.31 |
87.58 |
11.43 |
3.539 |
<RL |
<RL |
<RL |
0.9997 |
0.2846 |
|
B-d4
|
7.42 |
64.37 |
21.43 |
3.539 |
<RL |
<RL |
<RL |
0.9954 |
7.4969 |
|
S-13C3
|
8.17 |
61.67 |
9.553 |
3.539 |
<RL |
<RL |
<RL |
0.9950 |
0.1848 |
|
11DOC-13C3
|
12.01 |
114.2 |
10.33 |
3.539 |
<RL |
<RL |
<RL |
0.9996 |
0.9914 |
E |
E-13C3 |
— |
90.00 |
3.534 |
0.1035 |
0.9520 |
1.378 |
6.440 |
0.9998 |
0.9696 |
|
F-13C3
|
1.69 |
94.72 |
4.128 |
0.1035 |
0.7467 |
1.292 |
6.425 |
1.0000 |
1.6618 |
|
Ald-d4
|
1.74 |
88.09 |
15.60 |
0.1047 |
0.6650 |
0.9494 |
3.533 |
0.9998 |
7.1236 |
|
B-d4
|
5.8 |
91.33 |
19.45 |
0.1035 |
0.7505 |
1.168 |
7.764 |
1.0000 |
29.4480 |
|
S-13C3
|
6.55 |
89.77 |
3.692 |
0.1035 |
0.8860 |
1.304 |
6.276 |
1.0000 |
0.6868 |
|
11DOC-13C3
|
10.39 |
104.3 |
6.807 |
0.1035 |
0.8950 |
1.725 |
7.816 |
1.0000 |
6.1497 |
F |
F-13C3 |
— |
95.56 |
1.443 |
0.05613 |
1.494 |
3.825 |
9.066 |
0.9999 |
0.9108 |
|
E-13C3
|
1.74 |
90.06 |
4.115 |
0.05613 |
1.690 |
3.758 |
8.763 |
1.0000 |
0.5455 |
|
Ald-d4
|
3.45 |
93.38 |
15.61 |
0.05613 |
0.8798 |
2.154 |
4.725 |
1.0000 |
3.7853 |
|
B-d4
|
4.09 |
92.00 |
18.97 |
0.05613 |
1.531 |
3.486 |
10.93 |
0.9999 |
15.9360 |
|
S-13C3
|
4.84 |
89.09 |
3.344 |
0.05613 |
1.586 |
3.574 |
8.496 |
1.0000 |
0.3895 |
|
11DOC-13C3
|
8.68 |
104.6 |
6.532 |
0.05613 |
1.669 |
4.853 |
10.89 |
1.0000 |
3.3828 |
B |
B-d4
|
— |
92.79 |
18.85 |
0.8693 |
<RL |
<RL |
5.328 |
1.0000 |
3.7159 |
|
S-13C3
|
0.66 |
89.69 |
2.369 |
0.8693 |
<RL |
0.8997 |
4.183 |
0.9997 |
0.0905 |
|
F-13C3
|
4.2 |
101.4 |
2.717 |
0.8693 |
<RL |
<RL |
3.159 |
0.9999 |
0.2058 |
|
11DOC-13C3 |
4.5 |
106.0 |
4.482 |
0.8693 |
<RL |
1.379 |
5.397 |
0.9999 |
0.7883 |
|
E-13C3
|
5.92 |
96.74 |
2.540 |
0.8693 |
<RL |
0.9329 |
4.511 |
1.0000 |
0.1185 |
|
Ald-d4
|
7.63 |
93.85 |
15.73 |
0.8693 |
<RL |
<RL |
2.469 |
0.9998 |
0.8768 |
S |
S-13C3 |
— |
86.07 |
2.114 |
0.02738 |
0.1255 |
0.3834 |
5.969 |
1.0000 |
0.7621 |
|
B-d4
|
0.76 |
89.43 |
18.47 |
0.02738 |
<RL |
0.3413 |
7.630 |
1.0000 |
31.2410 |
|
11DOC-13C3
|
3.83 |
103.4 |
5.938 |
0.02738 |
0.04642 |
0.5206 |
7.660 |
1.0000 |
6.6189 |
|
F-13C3
|
4.87 |
98.57 |
5.013 |
0.02738 |
<RL |
0.3427 |
6.647 |
1.0000 |
1.6906 |
|
E-13C3
|
6.59 |
94.71 |
4.956 |
0.02738 |
0.1040 |
0.3834 |
6.636 |
0.9999 |
0.9812 |
|
Ald-d4
|
8.3 |
90.99 |
16.49 |
0.02738 |
0.04995 |
0.1790 |
3.372 |
1.0000 |
7.2227 |
11DOC |
11DOC-13C3 |
— |
83.18 |
3.491 |
0.3664 |
<RL |
<RL |
5.611 |
1.0000 |
1.6794 |
|
S-13C3
|
3.84 |
69.37 |
3.926 |
0.3664 |
<RL |
<RL |
4.441 |
0.9998 |
0.1899 |
|
B-d4
|
4.59 |
71.76 |
20.12 |
0.3664 |
<RL |
<RL |
5.504 |
0.9999 |
7.9127 |
|
F-13C3
|
8.7 |
74.12 |
5.565 |
0.3664 |
<RL |
<RL |
4.596 |
1.0000 |
0.4575 |
|
E-13C3
|
10.42 |
70.07 |
4.042 |
0.3664 |
<RL |
<RL |
4.598 |
0.9999 |
0.2668 |
|
Ald-d4
|
12.13 |
104.4 |
14.81 |
0.3664 |
<RL |
<RL |
3.466 |
1.0000 |
1.2503 |
DHEA |
11DOC-13C3
|
1.79 |
117.0 |
8.148 |
0.1082 |
<RL |
<RL |
<RL |
1.0000 |
2.7035 |
|
S-13C3
|
5.63 |
88.05 |
9.368 |
0.1423 |
1.618 |
1.194 |
0.4861 |
1.0000 |
0.3218 |
|
B-d4
|
6.38 |
71.36 |
22.96 |
0.06617 |
1.109 |
0.9804 |
0.5460 |
0.9997 |
17.3940 |
|
F-13C3 |
10.49 |
93.49 |
10.29 |
0.1351 |
1.141 |
1.179 |
0.4802 |
1.0000 |
0.7788 |
|
E-13C3
|
12.21 |
88.57 |
7.898 |
0.2530 |
1.739 |
1.260 |
0.5557 |
1.0000 |
0.4518 |
|
Ald-d4
|
13.92 |
83.47 |
15.52 |
0.1670 |
0.5932 |
0.5494 |
0.1800 |
1.0000 |
3.4153 |